Effect of ni core structure on the electrocatalytic activity of pt-ni/c in methanol oxidation.

Loading...
Thumbnail Image

Date

2013

Authors

Journal Title

Journal ISSN

Volume Title

Publisher

MDPI

Abstract

Methanol oxidation catalysts comprising an outer Pt-shell with an inner Ni-core supported on carbon, (Pt-Ni/C), were prepared with either crystalline or amorphous Ni core structures. Structural comparisons of the two forms of catalyst were made using transmission electron microscopy (TEM), X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS), and methanol oxidation activity compared using CV and chronoamperometry (CA). While both the amorphous Ni core and crystalline Ni core structures were covered by similar Pt shell thickness and structure, the Pt-Ni(amorphous)/C catalyst had higher methanol oxidation activity. The amorphous Ni core thus offers improved Pt usage efficiency in direct methanol fuel cells.

Description

Keywords

Electrocatalysts, Amorphous, Core-shell structure, Fuel cell, Methanol oxidation

Citation

Kang, J. et al. (2013). Effect of ni core structure on the electrocatalytic activity of pt-ni/c in methanol oxidation. Materials, 6: 2689-2700